Urea
Analyt: | Urea |
Matrix: | Serum, Urine |
Measuring Method: | GC-ID/MS |
Standard: | Urea NIST 912b |
Internal Standard: | ¹³C,¹⁵N₂-Urea |
Sample Processing: | Samples are spiked gravimetrically with internal standard, equilibrated, then precipitated with ethanol, centrifuged and the supernatant evaporated to dryness. Derivatisation is with Damdee solution in pyridine. |
Measurement: | Measurement at m/z 171 and m/z 174 |